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To find out the origin of dolomite, the precipitation of primary dolomite, and the formation of pores in dolomite, petrologic and geochemical characteristics of typical samples from Sichuan and Tarim Basin were analyzed based on the previous understandings, and three aspects of results were achieved. (1) A classification of dolomite origins based on petrologic features, forming environment, and time sequence was proposed, which shows clear boundaries of diagenetic and characteristic realms and evolved clues between different types of dolomite. (2) Petrographic and geochemical identification marks for different types of dolomite were presented, revealing that the orderly geochemical variation of different types of dolomite is the response to the change of forming environment of dolomite during continuous time sequence. (3) The contribution of dolomitization to the formation of porosity was re-evaluated, revealing that the porosity in dolomite was mostly attributed to the primary pores and supergene dissolution and burial dissolution, and early dolomitization was conducive to the preservation of primary pores. These understandings are of great theoretical significance for identifying the origins and types of dolomite, and can guide the prediction of dolomite reservoirs.
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Paleo-sedimentary environment of Chang 7 Member of Upper Triassic Yanchang Formation in Ordos Basin, including the paleoclimate, paleo-salinity and paleo-redox conditions were restored through geochemical elements analysis of 289 samples collected from the outcrop sections around and wells drilled in the basin and using a series of identification indexes of paleo-climate, paleo-salinity and paleo-redox conditions, such as CaO/MgO?Al2O3, Sr/Cu, Rb/Sr, Rb/K2O, Th/U, V/(V+Ni), the content of element B tested from the mudstone. Comprehensive analysis shows that in sedimentary period of the Chang 7, the paleo-climate was warm temperate to subtropical climate with temperature higher than 15 °C, the water body was continental brackish water to freshwater, and the sediments were deposited under strong reduction conditions. Suitable temperature, extensively deep lake basin and strongly reductive paleo-sedimentary environment led to the blooming, enrichment and preservation of organic matter in the submember Chang 73. As a result, a set of high-quality source rock was formed, laying material foundation for large-scale accumulation of shale oil.
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Migration and accumulation simulation of oil and gas in carrier systems has always been a difficult subject in the quantitative study of petroleum geology. In view of the fact that the traditional geological modeling technology can not establish the interrelation of carriers in three dimensional space, we have proposed a hybrid-dimensional mesh modeling technology consisting of body (stratum), surfaces (faults and unconformities), lines and points, which provides an important research method for the description of geometry of sand bodies, faults and unconformities, the 3D geological modeling of complex tectonic areas, and the simulation of hydrocarbon migration and accumulation. Furthermore, we have advanced a 3D hydrocarbon migration pathway tracking method based on the hybrid-dimensional mesh of the carrier system. The application of this technology in western Luliang Uplift of Junggar Basin shows that the technology can effectively characterize the transport effect of fault planes, unconformities and sand bodies, indicate the hydrocarbon migration pathways, simulate the process of oil accumulation, reservoir adjustment and secondary reservoir formation, predict the hydrocarbon distribution. It is found through the simulation that the areas around the paleo-oil reservoir and covered by migration pathways are favorable sites for oil and gas distribution.
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Alkaline-lacustrine deposition and its evolution model in Permian Fengcheng Formation at the Mahu sag, Junggar Basin were investigated through core and thin-section observation, geochemical and elemental analysis, logging response and lithofacies identification. Six lithofacies are developed in the Fengcheng Formation. The Feng 2 Member (P1f2) is dominated by lithofacies with alkaline minerals, while the upper part of the Feng 1 Member (P1f1) and the lower part of the Feng 3 Member (P1f3) are primarily organic-rich mudstones that are interbedded with dolomite and dolomitic rock. Paleoenvironment evolution of Fengcheng Formation can be divided into 5 stages, which was controlled by volcanic activity and paleoclimate. The first stage (the early phase of P1f1) was characterized by intensive volcanic activity and arid climate, developing pyroclastics and sedimentary volcaniclastic rocks. The secondary stage (the later phase of P1f1) had weak volcanic activity and humid climate that contributed to the development of organic-rich mudstone, forming primary source rock in the Fengcheng Formation. The increasing arid climate at the third stage (the early phase of P1f2) resulted in shrinking of lake basin and increasing of salinity, giving rise to dolomite and dolomitic rocks. The continuous aird climate, low lake level and high salinity at the fourth stage (the later phase of P1f2) generated special alkaline minerals, e.g., trona, indicating the formation of alkaline-lacustrine. The humid climate made lake level rise and desalted lake water, therefore, the fifth stage (P1f3) dominated by the deposition of terrigenous clastic rocks and dolomitic rocks.
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The development, evolution and formation mechanism of faults and their control on the migration and accumulation of Mesozoic oil and gas in the middle-shallow layers of the slope zone of Mahu sag were studied by the interpretation of seismic and drilling data. Two types of faults, normal and strike-slip, are developed in the middle-shallow layers of the slope zone of the Mahu sag and they are mostly active in the Yanshanian period. They are divided into four grade faults: The grade I strike-slip faults with NWW to near EW direction are related to the left-lateral transpressive fault zones in the northwest of Junggar Basin since the end of the Triassic. The grade II faults with NE to NNE direction are the normal faults located at the junction of the fault zone and the slope zone, and their formation is related to the extension at the top of the nose-like structures in the fault zone. The grade III faults, which are also the normal faults, are the result of the extension at the top of the lower uplifts in the slope zone and differential compaction. The grade IV faults with NE direction are normal faults, which may be related to the extension environment at the tip of the lower uplifts. Faults not only are the channel for the vertical migration of oil and gas, but also control the oil-gas accumulation. There are two types of oil-gas reservoirs in the middle-shallow layers of slope zone of Mahu sag: fault block reservoirs and fault-lithologic reservoirs. They have large traps and promising exploration potential.
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Based on geologic, seismic and drilling data of basins in China, the basic types of “truncation and onlap” unconformities are examined and their temporal and spatial variation and geologic significances are explored. The “truncation and onlap” unconformities and superimposing styles of overlying and underlying strata vary under different tectonic settings. Under extensional settings, there are three basic superimposing styles and unconformities, such as parallel superimposing style and unconformity with breaking outward, parallel superimposing style and unconformity with breaking inward, as well as superimposing and unconformity style with rotation. Under compressional settings, there are four basic types, such as overlap superimposing style and unconformity on fold, syn-depositional fold superimposing style and unconformity, anticline-syncline superimposing style and unconformity, as well as superimposing style and unconformity in overlap-filling incised valley on top of folds. “Truncation and onlap” unconformities always superimposed each other in space, and exhibit three kinds of superimposed unconformities, i.e., superimposed unconformities formed under continuous uplifting, under transition of uplifting, and under propagation of deposition center. They may also change with time too, i.e., tilting, rotating, folding, and migration. Controlled by the migration of basin depocenters, it is shown that there are unconformities formed under the transition of paleogeomorphy or subsidence center, under the migration of fault-sag, and under the slipping of detachment fault. “Truncation and onlap” unconformities are important positions for traps and significant pathways for hydrocarbon migration, and they are favorable sites for ore deposit and resources occurrence.
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Based on the core, cast thin section, whole rock analysis, conventional physical properties and high pressure mercury intrusion test, the sedimentary diagenesis characteristics of rudist shoal in Cretaceous Mishrif Formation of H Oilfield, Iraq and its control on the reservoir were studied. The rudist shoal of the Mishrif Formation develops in the high-stand systems tract and is distributed in the high places of paleogeomorphology on the edge of platform with strong hydrodynamic force. According to the relative sea level changes, lithologic evolution and sedimentary structure characteristics of the rudist shoal, the single rudist shoal is divided into four lithologic sections: A, B, C and D, that is, low-angle cross-bedding pelletoids-rudist packstone, low-angle cross-bedding and parallel bedding arene-rudist grainstone, parallel bedding rudist gravel limestone, and horizontal bedding carbonaceous mudstone. The complete sedimentary sequence of a single rudist shoal is often disrupted. Several rudist shoals superimpose to form thick rudist shoal sediment. The single rudist shoal thickness and lithologic sections assemblage change regularly in vertical direction. The rudist shoal has the characteristics of “strong dissolution, weak cementation and strong compaction”, forming pore-type reservoir with intergranular pores, intergranular dissolved pores, mold pores, and dissolved pores. With mainly coarse pore throats larger than 5 μm, the reservoir is of medium-high porosity and high permeability. There is lithological reverse cycles inside single shoals and between single shoals, with content of mud crystals decreasing from the bottom to the top, dissolution increasing, cementation decreasing in strength, pore throats getting larger, and physical properties turning better. The rudist shoal of MB2-1 at the top of the high-stand systems tract has the largest thickness, moreover, subject to the strongest atmospheric freshwater leaching, this layer has the most significant dissolution and the largest pore throat, so it is the best reservoir of the Mishrif Formation.
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Based on performance data of over 600 wells in 32 large gas fields of different types in China, the correlation is established between per-well average dynamic reserves ($\bar{G}$) and average initial absolute open flow potential ($\bar{q}_{IAOF}$) of each field, and its connotation and applicability are further discussed through theoretical deduction. In log-log plot, $\bar{G}$vs. $\bar{q}_{IAOF}$exhibit highly dependent linear trend, which implicates the compatibility between $\bar{G}$ and $\bar{q}_{IAOF}$ attained through development optimization to reach the balance among annual flow capacity, maximum profits and certain production plateau, that is to match productivity with rate maintenance capacity. The correlation can be used as analogue in new gas field development planning to evaluate the minimum dynamic reserves which meet the requirement of stable and profitable production, and facilitate well pattern arrangement. It can also serve as criteria to appraise the effectiveness and infill drilling potential of well patterns for developed gas fields.
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To explore the method of improving development effect and solving the problem of water breakthrough and water out for ultralow permeability fractured reservoirs, an indoor evaluation method of dynamic imbibition for fracture-matrix system was established taking the Chang 8 reservoir in southern Yanchang Oilfield as a research target. Key factors for the imbibition effect were obtained, an imbibition’s rate expression was obtained, a model considering the double effects of imbibition-displacement was built and optimal injection and production parameters for the research area were obtained as well. The results show that an optimum displacement rate that maximizes the oil displacement efficiency exists in the water displacing oil process, and the optimal displacing rate becomes smaller as the permeability decreases. The imbibition displacement efficiency increases as the reservoir quality index and water wettability index of rock become bigger. But the larger the initial water saturation or oil-water viscosity ratio is, the smaller the imbibition displacement efficiency is. The optimal injection-production ratio for the Chang 8 reservoir of southern Yanchang Oilfield is 0.95, and the predicted recovery is 17.2% when the water cut is 95%, it is 2.9% higher than the recovery of conventional injection-production ratio 1.2. By using the moderate water injection technique based on the double effects of imbibition-displacement mechanism, the water injection development effect for the ultra-low permeability fractured reservoirs can be improved significantly.
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Based on the similarity criterion, volcanic rock samples were taken from outcrops to make experimental models. Water flooding experiments of five-spot well pattern, nine-spot well pattern, five-spot to nine-spot well pattern, the relationship between relative well and fracture positions, and injection rate in dissolution vug-cave reservoirs with/without fractures were carried out to analyze variation regularities of development indexes, find out development characteristics of water flooding with different well patterns and sort out the optimal water flooding development mode. For dissolution vug-cave reservoirs without fractures, five-spot well pattern waterflooding has very small sweeping area, serious water channeling and low oil recovery. When the well pattern was adjusted from five-spot to nine-spot well pattern, oil recovery could be largely improved, but the corner well far from the injector is little affected. In dissolution vug-cave reservoirs with fractures, when the injector and producer are not connected by fractures, the fractures could effectively connect the poorly linked vugs to improve the development effect of water flooding. Whether there are fractures or not in dissolution vug-cave reservoirs, the development effect of nine-spot well-pattern is much better than that of five-spot well pattern and five-spot to nine-spot well pattern, this is more evident when there are fractures, and the edge well has better development indexes than corner well. At the high-water cut stage of water flooding with nine-spot well pattern, the oil recovery can be further improved with staggered line-drive pattern by converting the corner well into injection well. It is helpful to increase the oil production of corner well of nine-spot well pattern by increasing the injection rate, and improve ultimate oil recovery, but the water-free production period would be greatly shortened and water-free recovery would decrease.
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Waterflooding experiments were performed using Micro-CT on four cores of different pore structures from Donghe sandstone reservoirs in the Tarim Basin. The water, oil and grains were accurately separated by the advanced image processing technology, the pore network model was established, and parameters such as the number of throats and the throat size distribution were calculated to characterize the microscopic heterogeneity of pore structure, the flow of oil phase during displacement, and the morphology and distribution of remaining oil after displacement. The cores with the same macroscopic porosity-permeability have great differences in microscopic heterogeneity of pore structure. Both macro porosity-permeability and micro heterogeneity of pore structure have an influence on the migration of oil phase and the morphology and distribution of remaining oil. When the heterogeneity is strong, the water phase will preferentially flow through the dominant paths and the remaining oil clusters will be formed in the small pores. The more the number of oil clusters (droplets) formed during displacement process, the smaller the average volume of cluster is, and the remaining oil is dominated by the cluster continuous phase with high saturation. The weaker the heterogeneity, the higher the pore sweep efficiency is, and the remaining oil clusters are mainly trapped in the form of non-continuous phase. The distribution and morphology of micro remaining oil are related to the absolute permeability, capillary number and micro-heterogeneity. So, the identification plate of microscopic residual oil continuity distribution established on this basis can describe the relationship between these three factors and distribution of remaining oil and identify the continuity of the remaining oil distribution accurately.
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Gas-water-rock interactions during natural gas storage in a low permeability aquifer and main factors affecting the storage capacity were investigated in laboratory with core experiments. The results showed that gas injection flow rate had a major impact on stored gas volume and stored gas volume is higher at high flow rate. Gas storage volume ranged between 6%-20% of the pore space at experimental condition. Enhancing injection pressure can enhance gas storage volume. Statistics showed that injection flow rate had a greater influence on the gas storage volume than pressure. The retention time also had an impact on the gas storage process. Most of the natural gas was trapped in the reservoir and could not be produced after long time of retention. Atomic absorption spectroscopy indicated that ions concentrations of the brine and water evaporation increased when gas was injected into brine saturated core, and precipitation might occur, reducing porosity and permeability of core. Gas chromatography analysis showed that the concentration of carbon dioxide in the natural gas decreased and the concentration of methane increased after storage in the core.
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A novel laboratory simulation method for modeling multi-staged fracturing in a horizontal well was established based on a true tri-axial hydraulic fracturing simulation system. Using this method, the influences of net pressure in hydraulic fracture, stage spacing, perforation parameter, horizontal stress bias and well cementation quality on the propagation geometry of multiple fractures in a tight sandstone formation were studied in detail. The specimen splitting and analogy analysis of fracturing curve patterns reveals: Multiple fractures tend to merge under the condition of high horizontal stress bias and short stage spacing with pre-existing hydraulic fractures under critical closure situation, and the propagation of subsequent fractures is possibly suppressed because of high net pressure in pre-created fractures and asymmetric distribution of fracture width. And the subsequently created fractures are situated in the induced stress decreasing zone due to long stage spacing, leading to weak stress interference, and perforation with intense density and deep penetration facilitates the decrease of initiation fracture pressure. The deflection angle of subsequent fracture and horizontal stress variation tend to be amplified under low horizontal bias with constant net pressure in fractures. The longitudinal fracture is likely to be initiated at the interface of wellbore and concrete sample with poor cementation quality. The initiation fracture pressure of the different stages increases in turn, with the largest increase of 30%. Pressure quickly declines after initiation with low propagation pressure when the transverse hydraulic fracture is formed. The pressure reduces with fluctuation after the initiation of fracture when the fracture deflects, the extension pressure is high, and the fracture formed is tortuous and narrow. There is a violently fluctuant rise of pressure with multiple peak values when longitudinal fracture created, and it is hard to distinguish the features between the initiation stage and propagation stage.
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Drill string will sustain large uplift force during the shut-in period after gas overflow in an ultra-deep well, and in serious case, it will run out of the wellhead. A calculation model of uplift force was established to analyze dynamic change characteristics of the uplift force of drill string during the shut-in period, and then a management procedure for the uplift risk during the shut-in period after gas overflow in the ultra-deep well was formed. Cross section method and pressure area method were used to analyze the force on drill string after shut-in of well, it was found that the source of uplift force was the "fictitious force" caused by the hydrostatic pressure in the well. When the fictitious force is in the opposite direction to the gravity, it is the uplift force. By adopting the theory of annular multiphase flow, considering the effects of wellbore afterflow and gas slippage, the dynamic change of the pressure and fluid in the wellbore and the uplift force of drill string during the shut-in period were analyzed. The magnitude and direction of uplift force are related to the length of drill string in the wellbore and shut-in time, and there is the risk of uplift of drill string when the length of drill string in the wellbore is smaller than the critical drill string length or the shut in time exceeds the critical shut in time. A set of treatment method and process to prevent the uplift of drill string is advanced during the shut-in period after overflow in the ultra-deep well, which makes the risk management of the drill string uplift in the ultra-deep well more rigorous and scientific.
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The microstructures of shale samples before and after hydration were characterized by field emission scanning electron microscopy (FESEM), and the differences in microstructure and physical parameters of original shale samples, water saturated samples and samples with water centrifugated were examined by micro CT, porosity and permeability tests. The FESEM test shows that the hydration has no effect on the main morphology, position and pores of organic matter (OM). Hydration can increase the number and width of fractures in shale, including generation of new fractures and extension of existent fractures between inorganic minerals and width increase of fractures between banded organic matter and inorganic minerals. Micro CT results of samples with different water saturations show that the intensity of hydration is dominated by primary fracture development, in other words, the more developed the primary fractures of the shale, the stronger the hydration will be. The width of fractures increased two to five times by intense hydration. The porosity of shale is mainly controlled by organic matter content and secondly influenced by the fracture development. The permeability of shale is mainly affected by fracture development and secondly by the porosity. The fracture development influenced both porosity and permeability, but more strongly on permeability than porosity.
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Lost circulation is one of the most important concerns of the drilling industry, causing excessive expenditure and increasing the non-productive drilling time. In this study, various lost circulation materials (LCMs) were used to control the lost circulation of two types of drilling fluids, bentonite mud and a new eco-friendly mud, named RIA-X, which has a remarkable effect on decreasing the amount of lost circulation in fractured and highly permeable reservoirs. The Bridging Material Test (BMT) apparatus was used to investigate the effectiveness of various LCMs in fractures of various sizes and to select the LCM and combination with the best performance. The use of three-dimensional fractures is one of the most notable points of this work, which makes the experimental conditions similar to those of real wells. The lost control performance of the new eco-friendly LCMs in RIA-X mud was tested in field. The outcomes show that the designed LCMs are able to control severe lost circulation that regular processes such as cementing or drilling with foam cannot deal with.
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Based on the merged 3D seismic data, well logging, formation testing, analysis and testing data, the structural evolution, sedimentary reservoirs, thermal evolution of source rocks were investigated of Paleogene Kongdian Formation in the trough area of Cangdong sag, Bohai Bay Basin. A conventional-unconventional hydrocarbon accumulation pattern in the trough area of rifted basin was revealed. The reservoir forming elements in the trough area of Cangdong sag have a zonation feature in terms of reservoirs and source rocks. There are two types of reservoir forming models, primary trough and reformed trough. The formation and evolution of trough controlled the orderly distribution of conventional oil to unconventional oil in the trough. Particularly, structural reservoirs occur in the upper part of the trough, stratigraphic-lithologic reservoirs are likely to form in the delta front deposits at the outer ring of trough, the middle ring transitional belt is the favorable site for tight oil reservoirs, while the fine grain deposits zone in the inner ring is shale oil and gas exploration area. The study has pointed out the new domains and directions for searching reserves in the secondary exploration of mature oilfields.
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Based on GC-MS data of saturate and aromatic hydrocarbon fractions in crude oils from Well TD 2 and the Yingmaili and Tazhong area in the Tarim Basin, the end-member oil derived from Cambrian-Lower Ordovician source rocks was determined. The analytical results show that the crude oil from Well TD2 is rich in 3-6 ring polycyclic aromatic hydrocarbons without alkyl group, suggesting that this oil was altered by an abnormally thermal event. It contains a complete series of normal alkanes and 25-norhopanes, indicating that it is mixed oil of normal oil and biodegraded oil, so it can’t be taken as end-member oil derived from Cambrian source rocks. The geochemical characteristics of crude oils from Well TZ11 and TZ30 are completely different from the crude oils from Well YM101 and YM201 generated by Middle-Upper Ordovician source rocks, so it is inferred that they are derived from Cambrian-Lower Ordovician source rocks. In addition, these crude oils don’t contain 25-norhopanne series, indicating that they haven’t suffered biodegradation and satisfy with geochemical conditions of end-member oil. It is noteworthy that the two kinds of marine oils have similar triaromatic steroids and methyl triaromatic steroids, but very different C27-29 steranes and C28-30 methyl steranes, showing that they are not a good indicator of organic matter input. Triaromatic dinosteroids are a kind of biomarkers most usually used in marine oil-source correlation in the Tarim Basin, but the big differences in their relative abundances between crude oil from Well TD 2 and two kinds of end-member marine oils suggest that they are easily affected by thermal maturity and should be cautiously used in marine oil-source correlation.
