Petroleum Exploration and Development Editorial Board, 2020, 47(1): 12-29 doi: 10.1016/S1876-3804(20)60002-7

RESEARCH PAPER

Breakthrough of shallow shale gas exploration in Taiyang anticline area and its significance for resource development in Zhaotong, Yunnan Province, China

LIANG Xing,1,*, XU Zhengyu2, ZHANG Zhao1, WANG Weixu1, ZHANG Jiehui1, LU Huili2, ZHANG Lei1, ZOU Chen1, WANG Gaocheng1, MEI Jue1, RUI Yun1

1. PetroChina Zhejiang Oilfield Company, Hangzhou 311100, China

2. PetroChina Hangzhou Research Institute of Petroleum Geology, Hangzhou, 310023, China

Corresponding authors: E-mail: liangx85@petrochina.com.cn

Received: 2019-11-21   Revised: 2019-12-5   Online: 2020-02-15

Fund supported: Supported by the China National Science and Technology Major Project2017ZX05063

Abstract

Based on exploration and development results and evaluation of marine shale gas in South China in the past ten years, in view of the features of "high maturity, strong tectonic reformation and high shear stress" of the shale in Zhaotong exploration zone in the Yunnan and Guizhou Plateau, as well as the key issues of long time diffusion and leakage of shallow shale gas, and the preservation conditions, the factors controlling shallow shale gas sweet spot and key zone selection evaluation technology of shale gas are investigated. From 2017 to 2018, the first significant exploration breakthrough was made in the Taiyang anticline at a buried depth of 700 to 2 000 m, discovering large-scale proved geological reserves of shallow shale gas. By examining the accumulation conditions and sweet spot control factors of the shallow shale gas in this area, it is found that the accumulation and productivity potential of shale gas in the mountainous area with complex structure outside basin are controlled by five factors: (1) The gas-rich area has weak tectonic reformation and good preservation conditions on the whole, taking on typical anticline trap occurrence mode. (2) The gas-rich area is in over-pressure state and high in shale gas content. (3) The gas-rich area has high quality shale and thus superior source rock condition. (4) The gas-rich area has high quality reservoirs dominated by class I. (5) The shale gas reservoir in the gas-rich area has high content of brittle minerals and small difference between maximum and minimum horizontal stresses which are conducive to hydraulic fracturing. The innovative practice and core technologies formed during the exploration and production capacity construction of shallow shale gas in the Zhaotong demonstration zone have great reference significance for shallow shale gas exploration and development in other areas.

Keywords: shallow shale gas ; Silurian Longmaxi Formation ; Ordovician Wufeng Formation ; exploration breakthrough ; Taiyang anticline area ; Zhaotong area ; anticline

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Cite this article

LIANG Xing, XU Zhengyu, ZHANG Zhao, WANG Weixu, ZHANG Jiehui, LU Huili, ZHANG Lei, ZOU Chen, WANG Gaocheng, MEI Jue, RUI Yun. Breakthrough of shallow shale gas exploration in Taiyang anticline area and its significance for resource development in Zhaotong, Yunnan Province, China. [J], 2020, 47(1): 12-29 doi:10.1016/S1876-3804(20)60002-7

Introduction

In the past 10 years, inspired by the commercial development of shale gas in North America, a large number of shale gas geological surveys and drilling operations on the marine shale gas in South China have been carried out[1,2,3,4,5,6,7,8,9,10,11,12,13,14], and understandings and achievements on accumulation geological conditions including lithology, physical properties, gas content, geochemical, sedimentary and reservoir characteristics of shale, etc. have been obtained[1,2,3,4,5,6,7,8,9,10,11,12,13,14,15,16,17], and breakthroughs have been achieved in shale gas exploration in the middle-upper Yangtze area[10,11,12,13,14,15,16,17,18,19,20,21,22]. However, industrial development of shale gas is limited in the Sichuan-Chongqing demonstration zone in Sichuan Basin and Zhaotong, Pengshui demonstration zones near the Sichuan Basin, and the target layer is also lim-ited to the Upper Ordovician Wufeng Fm.-Lower Silurian Longmaxi Fm. The Longmaxi Fm. and other strata (Lower Sinian Doushantuo Fm., Lower Cambrian Qiongzhusi Fm., Carboniferous-Permian shale) in the periphery of Sichuan Basin have not been commercially developed yet. The shallow shale gas in this study refers to shale gas reservoir buried depth less than 2000 m, which is characterized by continuous distribution of sweet spot, high proportion of adsorbed gas, slight overpressure, low wellhead pressure and production, long production period, small horizontal stress difference, and good fracability. The shallow shale gas in this study is slightly deeper than the conventional shallow natural gas (less than 1500 m deep)[23] but shallower than the current commercially developed shale gas (sweet spot deeper than 2000 m)[24,25,26]. At present, the evaluation of development areas and commercial development of shallow shale gas are generally in the exploration stage, which has severely restricted the promotion of shale recovery technologies in China’s shale gas development demonstration zone and progress of commercial development of marine shale gas outside the Sichuan Basin. Based on the geological characteristics and shale gas exploration and development history inside and outside Sichuan Basin, China and the United States[15,16,17], and in consideration of the "over maturity, strong tectonic reformation and high shear stress" of the marine shale in South China, as well as key issues of long time diffusion and leakage of shallow shale gas, and difficult preservation in the complex structural conditions[17,18,19,20,21,22], the factors controlling marine shale gas formation and sweet spot in South China are taken as the keys in selecting shallow shale gas development area. Recently, breakthroughs have been made in shallow shale gas exploration in the Taiyang anticline area in the Zhaotong National Demonstration Zone, with more than 1000 ×108 m3 of proven geological reserves submitted. Based on analyzing formation conditions of shallow shale gas and controlling factors of sweet spot in the Taiyang anticline area of Zhaotong, the achievements in drilling and production, the evaluation criterion for selecting shallow shale gas sweet spot has been proposed, in the hope to provide guidance for evaluation and selection of marine shallow shale gas sweet spots in the Zhaotong demonstration zone and in the complex structural areas outside Sichuan and Chongqing and boost exploration and development of marine shale gas in South China.

1. Geological background

Recently, breakthroughs have been made in the shallow shale gas exploration in Taiyang anticline area in the northeast of Zhaotong demonstration zone, where the proven and controlled continuous gas-bearing area is about 580 km2. This area is characterized by the mountainous landforms in the Yunnan-Guizhou Plateau, and tectonically located at the transitional zone between the low-steep fold belt in the southern Sichuan basin and Dianqianbei depression (north) (Fig. 1). Marine and terrestrial shale gas strata are developed in the area[24, 27-28], among which the marine strata include Sinian, Paleozoic, and Middle-Lower Triassic, and the continental strata include Upper Triassic and Middle-Lower Jurassic, with a cumulative stratum thickness of 6000-7000 m. In addition, Triassic strata usually crop out of the surface. There are mainly three marine shale formations, including the Lower Sinian Doushantuo Fm., the Lower Cambrian Qiongzhusi Fm., and the Upper Ordovician Wufeng Fm.-Lower Silurian Longmaxi Fm, and Wufeng Fm.-Longmaxi Fm. are main shale gas exploration layers[26,29]. In the study area, the strata overlying the main exploration target reduce significantly in thickness compared to its periphery areas. The gas-rich shale generally has shallow burial depth, the buried depth of the main structure of the anticline is 500-1500 m, and the area with the buried depth < 2000 m accounts for 65% of the study area (Figs. 1 and 2).

Fig. 1.   Structural map of the bottom of Longmaxi Fm. and the distribution of shallow shale gas evaluation wells in Taiyang anticline area.


Fig. 2.   Correlation of Silurian-Triassic in northern Zhaotong demonstration zone.


The main target layer, Long11 sub-member is stable in the east-west direction but thins from north to south (Fig. 3). The Wufeng Fm. is composed of black graptolite shale and argillaceous shell limestone and has the small thickness of 2.0-6.0 m. The Long11 sub-member is made up of mainly black siliceous shale and carbonaceous shale, rich in pyrite and graptolite, and 20.0-40.0 m thick (Fig. 3). Based on lithology, electrical property, and graptolite fossil characteristics, Longmaxi Fm. is vertically divided into the 1st Member (hereinafter referred to as Long-1 Member) and the 2nd Member (Long-2 Member). Long-1 Member is further subdivided into 1st sub-member (Long-11) and 2nd sub-member (Long-12). The Long11 sub-member is divided into Long-111, Long-112, Long-113, and Long-114 sublayers (Fig. 4). Long-111 shale is rich in silicon and carbon[30,31,32,33] and 2.0-3.0 m thick. Long-112 shale has high silicon and carbon contents[30,31,32,33] and is 4.0-7.0 m thick. Long-113 shale has high silicon content and medium carbon content[30,31,32,33] and is 9.0-11.0 m thick. Long-114 shale has medium silicon and carbon contents[30,31,32,33] and is 12.0-16.0 m thick. All the sublayers basically thin from northwest to southeast (Fig. 3).

Fig. 3.   Shale thickness and lithofacies paleogeography of Long-11 sub-member of Longmaxi Fm. in Zhaotong demonstration zone.


Fig. 4.   Composite stratigraphic and sedomentary column of Wufeng Fm.-Longmaxi Fm. in Y105 well.


Regional stratigraphic correlation shows that the Wufeng Fm. in the demonstration zone is 5 m (YS108 well) to 10.8 m (YS128 well) thick in the west, 1.8 m (Y107 well) to 4.59 m (YS109 well) thick in the east, and 10.0 m (YS203 well) to 26.33 m (YQ8 well) thick in the south, and 1.8 m (Y107 well) to 4.59 m (YS109 well) thick in the north, indicating it is thinnest in the Taiyang anticline area. The main target layer, the Long-11 sub-member shale of the Longmaxi Fm. is relatively stable in thickness with little change, but it is thicker in the study area (30-40 m, Fig. 3). The overlying Long-12 sub-member is 95.46 m (YS112 well) to 143.33 m (YS111 well) thick in the west, 68.13 m (Y102 well) to 78.4 m (Y105 well) thick in the east, and 68.13 m (Y102 well) to 78.4 m (Y105 well) thick in the north, and 41.99 m (Shuangqiao) to 55.55 m (YS203 well) thick in the south, and it is thinnest in the Taiyang anticline area. The Long-2 Member is similar in characteristics with Long-12 sub-member (Fig. 2). The Lower Permian Qixia Fm. and Maokou Fm., the Lower Triassic Feixianguan Fm. and Jialingjiang Fm. all show a thinning trend towards the Taiyang anticline area. The Tongjiezi Fm. below the Lower Triassic Jialingjiang Fm. is dominated by argillaceous rocks, and varies to argillaceous limestone and merges with the Jialingjiang Fm. in the east Taiyang anticline area. The Upper Permian Emeishan Fm. basalt wedges out from west to east, and the Lower Silurian Hanjiadian Fm. thins most significantly (Fig. 2). It can be seen that the Long-1 1 sub-member shale is shallow in burial depth in the Taiyang anticline area (less than 2000 m in most part).

According to the data of 21 shale gas evaluation wells (Fig. 4), the sea level in the study area rose two times and fell two times during the sedimentary period of Longmaxi Fm.[31,32,33]. The first transgression occurred in the sedimentary period of Long-111 and reached the maximum marine flooding surface at the end of the period. The regression happened in Long-112, Long-113 and Long-114 sedimentary periods, and the high level occurred at the end of Long-114. The second transgression occurred in the sedimentary period of Long-12 sub-member, and reached the maximum marine flooding surface at the end of this period. The regression occurred in the sedimentary period from the Long-2 Member to the bottom of the Shiniulan Fm., and high stand systems tract occurred at the end of this period. The two times of sea level fluctuation show a rapid rise in the transgressive period and a slow decline in the receding period, reflecting the history of early transgression and late regression of the Longmaxi Fm.

The Late Ordovician to Early Silurian was a transitional period of sedimentary-structural evolution of the Yangtze Block. The study area was in the Sichuan, Chongqing-Hunan and western Hubei Caledonian foreland basin area held between the Jiangnan-Xuefeng orogenic belt formed in Caledonian orogeny in the south-east of the Yangtze Block and the middle Sichuan paleo-high in the northwest part. As the global sea level rose, the carbonate platform before the Late Ordovician was submerged, and the study area turned into epeiric sea type, water-retention deep-water shelf-reduction sedimentary environment, which provided good conditions for the reproduction of rich organic matter dominated by graptolite for Upper Ordovician Wufeng Fm. black shale and the Silurian Longmaxi Fm. black shale. In the early sedimentary period, the Longmaxi Fm. was dominated by terrigenous clastic rock, and the provenance was mainly from the Yunnan ancient paleo-land in the west part of the demonstration zone and the Qianzhong paleo- land in the south (Figs. 1 and 3). The Long-11 and Long-12 sub- members are dominated by a set of dark graptolite-bearing shale stably distributed, representing products under reduction conditions. In the late period, with the uplift of the southern paleo-land, regression occurred in the sedimentary period of the Long-2 Member, and gray shale and limestone interbeds of shelf facies developed. After the deposition of Longmaxi Fm., the sedimentary center of the study area gradually moved northward, and lithological differentiation occurred. In southeastern Sichuan area, Xiaoheba Fm. fine sandstone deposited[34], which turned westward and southward to the Lower Silurian Luoreping Fm. siltstone and limestone, or the Shiniulan Fm. biolithic limestone and the marl intercalated with the shale facies. In the sedimentary period of the Middle Silurian Hanjiadian Fm., gray-green-gray sandy shale and sandstone deposited, with commonly purple-red shale at the bottom, which generally reflects the gradual regression of sea water. By the end of the Middle Silurian, the study area completely exposed out of water. Regional geological surveys show that the Silurian is in unconformable contact with Permian in the Taiyang anticline, and the Upper Silurian to Carboniferous strata are missing, indicating that the area suffered wide denudation[35]. After the Hercynian period, the Taiyang anticline area received Upper Paleozoic and Mesozoic sediments gradually.

2. Major breakthrough in shallow shale gas exploration

The Zhaotong demonstration zone is in the Wumeng Mountain area at the juncture of Yunnan, Guizhou and Sichuan. The main part is in the Dianqianbei depression (Fig. 1) in the periphery of the southern Sichuan Basin. The shallow shale gas exploration here started back in 2009, when Well YQ1, the first shale gas geological survey well was drilled at the beginning of the construction of the demonstration zone[24]. As on one hand, the exploration area has complex structural geology and geographical conditions, making drilling and production of the medium-deep shale gas and factory-like operation more difficult and engineering investment and costs rise constantly[25,26], on the other hand, shale gas occurs in the micro-nano pores in the poorly-connected shale reservoirs, it was considered that although the shallow buried marine shale gas in the study area had some vertical dissipation, under the sealing of the direct tight caprock, the shallow shale reservoir might still had some gas retained, in April 2017, Y1 well and Y102 well in the Taiyang anticline area with favorable shale gas enrichment and preservation conditions were rechecked for shallow shale gas layers at buried depth of less than 1 000 m (Fig. 1). The Long-111 and Long-113 sublayers (at the burial depth between 768.5-778.8 m and 976.2-986.0 m respectively) in the Long-11 sub-member were volume fractured and tested for gas, obtaining an industrial gas flow of over 1 × 104 m3/d, making a breakthrough in shallow shale gas exploration in the Zhaotong demonstration zone, and verifying the exploration potential of shallow shale gas in the mountainous area with complex structure. Based on the success of the above two old wells and re-evaluation of previous results of exploration in shallow shale gas in South China, two new evaluation wells of Y103 and Y105 (vertical wells) were deployed in the Taiyang anticline at the end of 2017, and they also obtained industrial gas flow after fracturing (Table 1). Productivity evaluation continued in early 2018, horizontal well of Y102H1-1 targeting Long-11 sub-member was drilled for productivity evaluation, which was tested a high production gas flow of 5.6 × 104 m3/d.

Table 1   Statistics on fracturing test results of shallow shale gas in Taiyang anticline area.

Well typeWell nameTested layerDepth (Measured depth)/mTested production/
(104 m3•d-1)
Horizontal length/mAllocated production/(104 m3•d-1)Cumulative gas production/104 m3Pressure coefficient
VerticalY1Wufeng Fm.-Longmaxi Fm.976.2-986.00.390.3556.41.22
Y102Longmaxi Fm.768.5-778.81.120.8046.11.43
Y103Wufeng Fm.-Longmaxi Fm.1 074.0-1 088.00.800.5022.31.25
Y105Longmaxi Fm.1 685.0-1 693.82.061 1211.70108.41.29
HorizontalY102H1-1Wufeng Fm.-Longmaxi Fm.963.0-1 695.06.257452.67356.5
Y102H1-41 135.0-2 045.06.909103.60
Y102H1-51 006.0-1 906.04.109003.50
Y104H1-4Wufeng Fm.-Longmaxi Fm.1 253.0-1 509.014.101 013
Y107H1-2Wufeng Fm.-Longmaxi Fm.1193.7-1 120.411.42689
Y102H7-1Wufeng Fm.-Longmaxi Fm.1 790.0-2 772.015.12982
Y102H7-31 380.0-2 361.014.34981
Y105H1-2Longmaxi Fm.1 798.0-2 040.05.301 1213.90
Y108H1-1Longmaxi Fm.1 667.9-1 833.76.881 2252.80

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After comprehensive shallow shale gas development area selection and target evaluation and upgrade of engineering technologies, 6 wells in 3 well-pad in the Taiyang anticline area were put into production test to evaluate their productivity in 2018. After further optimization of evaluation design and drilling engineering technology integration, 13 wells have been tested after fracturing, and all of them have obtained high industrial gas flow (Table 1).Analysis of field test and well test data (Tables 1-2 and Figs. 1-3) shows that the shale gas producing layers in the study area are vertically continuous and laterally stable and have no interlayers. Vertically, the shale gas producing layers are concentrated in Wufeng Fm. to the bottom of Long-1 Member, and the Long-11 sub-member has higher gas production than the Wufeng Fm. Laterally, the area with high-silicon content and carbon-rich shale and the anticline high point area have the highest production.Compared with the medium-deep shale gas in Huangjinba-Zijinba area which have put into development in the demonstration zone, the shallow shale gas in the Taiyang anticline area has five characteristics. a) Shallower burial depth and higher adsorbed gas content: the shale gas layers are generally 500-2000 m deep, and have a total gas content of 3.81-5.34 m3/t, 4.3 m3/t on average, which is similar with the medium-deep shale gas (4.4-5.9 m3/t). The gas is dominated by methane, with a methane content of 91.19%-98.98%, 95.94% on average. The gas has a dry coefficient C1 /C1-5 of 0.9866- 0.9986, 0.9939 on average, indicating the gas is typical dry gas in the over-maturity stage. The gas layers have higher adsorbed gas content of over 50% (Table 2), indicating the free gas in the shallow shale has significant dissipation. b) Slight overpressure: The gas layers have pressure coefficients of 1.2-1.6 generally, indicating slight overpressure. The wells with shale gas reservoir at the buried depth of 700-2000 m have wellhead pressures of 6-12 MPa, and wells with shale gas reservoir at the buried depth of over 2000 m have wellhead pressures of more than 20 MPa. c) Big thickness, stable distribution and good fracability: The shale layers with TOC over 1% are 50.3-57.0 m thickness, free of interlayer, continuous vertically and stable in lateral distribution; the shale layers have a brittleness index of 50%-65%, and porosity of 4%-9%, 5.67% on average, matrix permeability of 0.000 017- 0.044 353×10-3 μm2, permeability of (0.015 246-6.178 450)× 10-3 μm2 in fracture-rich area, representing the physical properties of medium-low porosity and ultra-low permeability; the shale layers have horizontal stress difference of 4-15 MPa, which is obviously lower than the medium-deep shale layers (15-25 MPa), so the shale has better fracability. d) Lower initial production of wells: Test data shows vertical wells and horizontal wells in these reservoirs have a production of (0.5-2.0)× 104 m3/d and (2.63-20.70)×104 m3/d, respectively, and the wells produce stably at (2-5)×104 m3/ d in the initial stage. e) Stable production and low decline rate: Wells in the shallow shale gas reservoirs have a decline rate between 30% and 40% in the first year and long production life of over 30 years from prediction.

Table 2   Comparison of components and contents of shallow shale gas in Taiyang anticline area and the medium-deep shale gas in Huangjinba-Zijinba.

TypeBlockWell
name
Depth/mComponents/%Contents/(m3•t-1)Formation pressure coefficient
CH4C2H6C3H8CO2N2HeTotal gas contentFree gasAdsorbed gas
Shallow gasTaiyangY102772.29-772.5991.190.6400.148.010.013.811.482.331.43
Y1031 086.69-1 086.9696.671.3100.111.9104.352.052.31.25
Y1041 202.12-1 202.4096.881.0900.061.9704.152.042.111.29
Y1051 691.74-1 691.9996.620.6800.062.6405.343.002.341.29
Y1071 255.25-1 255.5197.64000.242.1205.072.672.401.37
Y1081 639.59-1 639.8696.630.1600.053.160
Average95.940.6500.113.300
Medium-deep gasHuangjinbaYS1082 498.2-2 499.398.360.2400.131.2705.23.71.61.96
YS1112 386.4-2 392.696.820.4700.142.5704.42.61.81.80
Ning 201
well block
N 2012 504.0-2 525.098.710.530.010.40.3505.84.01.82.03
ZijinbaYS1122 455.1-2 456.698.350.5100.091.0505.73.81.91.70
YS1152 254.8-2 256.397.610.7400.191.4605.94.11.81.70
Average98.000.4900.191.1.320

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3. Enrichment and high production of shallow shale gas

3.1. Weak structural transformation in gas-rich area with sealing caprock and good preservation condition

3.1.1. Developed caprock in shale gas area

The Silurian system exposes out of surface in the core area of the Taiyang anticline structure. The residual stratum overlying the main target reservoir of Long-11 sub-member is only 500 m thick. The residual strata increase from Long-12 sub-member, the Silurian Shiniulan Fm. and Hanjiadian Fm. at the core of the anticline to the Permian and Triassic at the flank of the study area, and increase in thickness from 800 m to more than 1500 m. Among them, the Shiniulan Fm. + Hanjiadian Fm. is a set of gray-dark and gray marlstone, gray-green and green-gray mudstone, and gray mudstone intercalated with argillaceous siltstone and brown-gray limestone, with wide distribution area and large cumulative thickness (600-900 m), and it acts as the regional cap and keeps the temperature and pressure field stable for the gas-bearing shale of the Wufeng Fm.-Long-11 sub-member in the study area[31, 36-40].

3.1.2. Developed shale reservoir with overall sealed system

The roof and floor of the gas reservoir of the Wufeng Fm.-Long-11 sub-member depositing continuously with the shale gas layers (Figs. 2 and 4) are characterized by tight lithology, large thickness, stable distribution, high breakthrough pressure, and good sealing property. The roof is the Long-2 Member gray-dark and gray medium-thick limy mudstone, argillaceous marlstone or siltstone, and argillaceous siltstone interbedded with thin layer silty mudstone, with an average porosity of 3.8% and an average permeability of 7.69 × 10-8 μm2. The floor is gray nodular marl, cryptocrystalline and micrite limestone of the Ordovician Linxiang Fm. and Baota Fm. with an average porosity of 1.58% and an average permeability of 0.0017×10-8 μm2. According to the physical properties, both the roof and floor of the shale reservoir are low-porosity, ultra-low permeability tight formations, which have provided good sealing and preservation for shale gas during formation of the shale gas reservoir and in the later tectonic reformation[31, 37].

3.1.3. Weaker tectonic reformation in late stage

The study area shows an anticline structural pattern of "sag around uplift" (Fig. 1), which is characterized by "inherited fold deformation and multi-stage weak fault reformation". Specifically, anticlines and synclines are adjacent to each other, and the structures are the Xuyong syncline, the Taiyang anticline, the Yunshanba syncline, the Baiyangping syncline, and Haiba anticline from north to south in the study area. The faults of multiple directions and orders superimpose, and the near EW reverse faults and near NS strike- slip faults take the majority[28,41].Taiyang anticline started to develop in the Caledonian period. After the Indosinian period, affected by the NS compression stress, it became a near EW trending anticline, with near EW trending thrust faults formed at the top and flanks. With continuous compression after the Yanshanian period and compressional strike-slip in Himalayan period, the anticlinoria deformed further progressively, and the early near EW anticlinoria was superimposed and reformed by the near NS compression-shear strike-slip fault. The complete EW anticlinoria was divided into two blocks, meanwhile, north-south trending small faults were formed in the south and north flanks of the anticline, but the anticline structure remained intact (Fig. 5). Although the Wufeng-Longmaxi shale experienced uplift, the strike-slip-thrust faults cutting the top have remained in compressed state, the tight rock layers on both sides of the fault juxtapose well, keeping the fault in good sealing, and the anticline of the target layer has maintained complete. The Silurian Shiniulan Fm. has conventional gas and the shale gas layer in the Longmaxi Fm. has overpressure, indicating that the anticline structural area has good preservation conditions and is a 3D overall closed system.

Fig. 5.   NE-SW seismic cross-section through wells in Taiyang anticline area (location of the cross-section is shown in Fig. 1).


3.1.4. Relatively complete anticline structure

According to statistics of wells of Y1, Y102, Y103, Y104, Y105, Y102H1-1, YS109, YS117, and YS118 which have made breakthroughs in the study area (Table 1 and Table 2), all gas-producing wells are in the Taiyang anticline trap, and wells in the anticline core have higher yield and wells in the anticline edges have slightly lower yield. Comprehensive analysis of logging and seismic data shows that the stratigraphic dips in the study area are complex and vary widely. The stratigraphic dips are 0°-10° in the anticline core, 10°-15° in the south flank and 15°-40° in the north flank in general, indicating the anticline is asymmetric in shape with a steep slope in the north and a gentle slope in the south (Figs. 1 and 5). Based on analysis of fine interpretation map and coherence map of 3D seismic data (Fig. 6), the faults in the study area are divided into II, III, and IV 3 orders, in which there are 2 faults of II order (with fault throw of over 1 km and longer extension), 4 of III order (with fault throw mainly between 80-300 m and longer extension), and 17 of IV order (with fault throw mainly between 20-80 m and short extension). The faults are largely III and IV compressive reverse faults with good sealing performance. Only 1 IV normal fault is open (F4-15 fault in the east, Fig. 6). The faults have been in a state of compressive-shear stress, and the rocks juxtaposing on both sides of the faults are tight marlstone and limestone, so the faults have good lateral sealing. The geological logging and test of cores from wells drilled on both sides of faults show high gas content; fracturing test of the shale gas reservoir shows high production and formation pressure coefficient of more than 1.2; conventional gas overflow is commonly observed during drilling of the overlying Shiniulan Fm., all indicating that the anticline has few faults, gentle strata in the main part, and good sealing performance on the whole. The sweet spot has the enrichment mode of typical compression-shear anticline gas reservoir (Fig. 7).

Fig. 6.   Distribution of faults at the bottom of Wufeng Fm.-Longmaxi Fm. in the study area.


Fig. 7.   Shallow shale gas accumulation and occurrence pattern in Taiyang anticline.


3.2. The gas-enrichment area with high in gas content

According to statistics of gas content of the cores from the Wufeng Fm.-the Long-11 sub-member of exploration wells in the study area (Fig. 8), the main target layers in the area have shale gas contents of 1.31-6.18 m3/t in general, 3.03 m3/t on average. Long-111 sublayer has the highest gas content of 6.00 m3/t on average, Long-112 sublayer comes second with 4.90 m3/t, Long-113 sublayer is the third with 3.95 m3/t, and Long-114 layer has the lowest gas content of 3.32 m3/t on average. Wufeng Fm. has an average gas content of 4.49 m3/t. Calibrated with the gas content data from gas desorption in drilling site, the gas content of shale gas target reservoir in the study area predicted by seismic attribute inversion under well log-seismic constraint is 3.30-5.51 m3/t, 4.27 m3/t on average (Fig. 9). The study results show that the shale gas reservoirs are continuously distributed in the study area, showing the characteristics of large-scale monolithic gas reservoir with large-scale gas accumulation.

Fig. 8.   Distribution of measured gas content of the shale sublayers in Wufeng Fm.-Long-11 sub-member in the study area.


Fig. 9.   Distribution of shale gas content of Wufeng Fm.-Long-1 1 sub-member in the study area.


According to the law of effective stress, the effective stress is uniform under the same porosity. The acoustic logging log can be used to quantitatively calculate the abnormal formation pressure in the study area. The formula of the equilibrium depth method is:

$p_{z}=\rho_{r}gz+\frac{(\rho_{r}-\rho_{w})g}{c}ln\frac{\Delta t}{\Delta t_{0}}$

Single well formation pressure is calculated by first calculating the original acoustic time difference Δt0 and the compaction coefficient c from the normal compaction curve of mudstone, and then the formation pressure is calcualted by using the acoustic difference of specific well. This method was used to calculate pressure of gas layers in 9 wells (Table 3). In combination with the prediction results of the 3D seismic attribute inversion in the study area, it can be seen that the shale gas layers in the main target formation of the Taiyang anticline zone are all in a critical overpressure state (Fig. 10).

Table 3   Statistics on pressure coefficients of the shale gas layers of Wufeng Fm.-Long-11 sub-member in the study area.

Well nameDepth/mPressure calculated with the
equilibrium depth method
Pressure coefficient from logging
Calculated pressure/
MPa
Hydrostatic pressure/
MPa
Pressure
coefficient
Y1948-97311.579.481.22(Measured)1.20
YS1361 978-2 01431.6719.961.62(Measured)1.68
Y102740-78010.817.521.431.46
Y1031 051-1 68913.2410.591.251.40
Y1051 663-1 69321.5016.611.291.40
YS1172 298-2 32936.3522.901.581.65
YS1182 229-2 26235.9022.201.611.60
YS1162 211-2 31736.3022.761.591.60
YS1092 170-2 20334.0821.641.571.51

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Fig. 10.   Distribution of pressure coefficients of the shale in Wufeng Fm.-Long-11 sub-member in the study area.


3.3. High-quality shale in gas-enrichment area

Affected by the Xuefeng-Qianzhong uplift event at the southern margin of Yangtze block in the Caledonian period, the study area entered the deep-water continental shelf deposition stage of the foreland occlusion bay basin in the early Silurian[28-29, 35] (Fig. 3) and had relatively quiet water in lag anoxic-dysoxic environment, where the planktonite fauna developed, which was favorable for enrichment of organic matter and formation of source rock. The dark argillaceous source rock layers (TOC≥1.0%) in the study area are widely distributed with large thicknesses typically between 60-180 m. The organic-rich shale (TOC≥2%) is concentrated at the bottom of Wufeng Fm.-Longmaxi Fm. and generally 30-40 m thick (Figs. 2-4). Analysis of 17 samples from the Wufeng Fm.-Long-11 sub-member in wells of YS109 and YS117 shows the samples have a saprolite content of 62%-86%, 77.95% on average in the kerogen maceral, Type II1 organic matter, and high vitrinite reflectance (Ro) generally between 1.99% and 3.08% with the average of 2.41%, indicating they are in the over maturity-dry gas stage. Although the source rock has passed the main hydrocarbon generation period (Fig. 11), and the source rock has experienced pyrolysis and cracking gas generation peak in the shale burial and reformation period, and most of generated hydrocarbon gas has retained in the shale source rock. In addition, the Taiyang anticline had a prototype of underwater paleo-uplift in the Sinian Period and the anticline has developed successively and remained in good sealing from Caledonian-Indochina period to now, so it has become a self-generation and self-storage sweet spot enrichment area[36,37,38,39].

Fig. 11.   Hydrocarbon generation history of Wufeng Fm.-Longmaxi Fm. source rock of Y105 well in the Taiyang anticline.


The organic carbon content of Wufeng Fm.-Long-11 sub-member in the study area calculated with log data after calibration with core analysis and test results is 0.42%-9.05%, averages at 2.92%. Vertically, Long-111 sublayer has the highest TOC between 2.40%-9.05%, 5.24% on average, Long-112 sublayer and Wufeng Fm. follow with 2.49%-5.58%, 3.53% on average, and 0.42%-5.82%, 3.68% on average respectively, and Long-113 and Long-114 sublayer have the lowest TOC between 1.83%-3.97%, 2.71% on average, and 1.15%-3.28%, 2.33% on average, respectively.

Comprehensive prediction of organic carbon content by combining the core analysis results, well logging calculation, and 3D seismic attribute inversion shows the Wufeng Fm.-the Long-11 sub-member in the study area has stable TOC between 2.54%-3.14%, 2.92% on average (Fig. 12), which means the shale layers reaches the TOC criterion of Types I+II high-quality reservoirs, and the material basis for hydrocarbon generation is good[29,31,36-37].

Fig. 12.   Distribution of total organic carbon of Wufeng Fm.- Long-11 sub-member shale in the study area.


3.4. The gas-rich areas with shale reservoirs dominated by Type I

The shale reservoirs in the Wufeng Fm.-Long-11 sub- member in the study area have fairly good physical properties, with a measured porosity of 2.92%-8.01%, 4.98% on average (Fig. 13), and logging interpretation porosity of 3.52%-5.96%, 4.29% on average (Fig. 14). Long-1 11 sublayer has the highest porosity, with an average measured value of 6.40% and average log interpretation value of 5.28% (Fig. 14), which are in good consistent with the porosity of 3.98%-5.41%, 4.29% on average from seismic inversion (Fig. 15). The shallow gas reservoirs are characterized by low porosity and low permeability, which is similar with the middle-deep shale gas reservoirs. Storage space in the reservoirs includes organic pores, inorganic pores, and micro-fractures.

Fig. 13.   Histogram of measured porosity of the shale layers in Wufeng Fm.-Long-11 sub-member in the study area.


Fig. 14.   Histogram of logging interpretation porosity of the shale sublayers in Wufeng Fm.-Long-11 sub-member in the study area.


Fig. 15.   Distribution of average porosity of Wufeng Fm.- Long-11 sub-member in the study area.


Organic pores are the main matrix storage space, and inorganic pores are dominated by dissolved pores and intergranular pores[31,40] (Fig. 16). The shale reservoirs have total pore specific surface areas of 15.5-31.7 m2/g, total pore volumes of 0.024-0.037 ml/g, and average pore sizes of 7.2-10.4 nm. Pore specific surface areas of the sublayers in decrease order are Long-111, Wufeng Fm., Long-112, Long-113, and Long-114. The shale pores size are mainly 2-50 nm, and meso-pores account for 87.32% of all pores and is the dominant pore type for shale gas adsorption and storage in the target reservoir. Fractures in the shale reservoirs are dominated by micro-fractures. The shale reservoirs also have some horizontal fractures and high-angle fractures, which are generally less than 30 cm long and some filled by pyrite and calcite (Fig. 17). The gas-rich shale sections have horizontal fractures, such as interlaminar seams and layer sliding joints (Fig. 17), are concentrated at the bottom of the Wufeng Fm.-Long-11 sub-member.

Fig. 16.   Pictures of organic pore, inorganic pore, and micro-fracture of Long-11 submember in the study area.


Fig. 17.   Pictures of fractures of Long-11 sub-member shale in the study area.


According to analysis of imaging log data, the shale reservoirs of the Wufeng Fm.-Long-11 sub-member in the study area have NNE-SSW fractures, and most of the fractures are medium and high angle ones. These are in consistent with the characteristics of fractures and faults predicted by seismic data (Fig. 18). Considering that the main part of the study area is the Taiyang anticline structure, dense micro-fracture systems are generally developed in the high parts of the anticline structure under continuous compression (Figs. 17 and 18), and some are subtle micro-fractures and fissures invisible for the naked eye. These micro-fractures and fissures reduce the horizontal stress difference of the shale and connects micro-nano pores during the reservoir fracturing, forming complex man-made fracture networks to achieve volume fracturing. This is possibly an important reason for the stable gas production of shale gas wells in the shallow part of the anticline structure.

Fig. 18.   Fractures predicted by ant tracing of Wufeng Fm.-Longmaxi Fm. shale in the study area.


According to the criterion for shale gas reservoir in the Sichuan-Chongqing demonstration zone of PetroChina[42] (Table 4), the Wufeng Fm. and Long-111, Long-112, and Long-113 sublayers of the Longmaxi Fm. in the study area are evaluated as Type I reservoirs, and Long-114 sublayer is evaluated as Type II reservoir. The reservoir characteristics of the sublayers in Wufeng Fm.-the Long-11 sub-member were evaluated comprehensively by combining the seismic attribute inversion and logging interpretation results. The sublayers with the area of Type I and Type II reservoirs in descending order in the study area are Long-111, Wufeng Fm., Long-112, Long-113, and Long-114 (Fig. 19), and Type I reservoirs of Wufeng Fm., Long-111, and Long-112 cover the main part of the Taiyang anticline, Long-113 and Long-114 cover most of the anticline area, and Type II reservoir cover other areas, indicating that the shale reservoirs of the main target formation in Taiyang anticline area have good quality and provide enough space for shale gas accumulation and are ideal places for shale gas accumulation and storage.

Table 4   PetroChina’s quality evaluation criterion for shale gas reservoir of Wufeng Fm. and Longmaxi Fm. in the Southern Sichuan Basin[42].

ParameterTOC/%Total
porosity/%
Total gas
content/(m3•t-1)
Brittleness index
Type I≥3≥4≥3≥55
Type II2-33-42-335-55
Type III1-22-31-2≤35

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Fig. 19.   Planar evaluation maps of Type I and II reservoirs of Wufeng Fm. and Long-1 1 sub-member in the study area.


3.5. The gas-rich area has shale engineering-geological conditions favorable for SRV fracturing

According to statistics on mineral composition of the Wufeng Fm.-Long-11 sub-member in the study area, the main mineral components are quartz, feldspar, carbonate, pyrite, and clay minerals, etc., and the measured content of brittle minerals (including quartz, feldspar, calcite, and dolomite) is 70.2% on average (Fig. 20), and 71.6% on average from logging. Generally, Long-111, Wufeng Fm., and Long-112 have higher brittle mineral contents, while Long-113, and Long-114 sublayers have lower brittle mineral content. Long-111 has a brittle mineral content of 74.0% from measurement and 75.16% from logging interpretation.

Fig. 20.   Histogram of measured brittle mineral contents of the shale sublayers in the Wufeng Fm.-Long-11 sub-member of the study area.


By combining seismic attribute inversion and logging interpretation, the brittle mineral contents of Wufeng Fm.- Long-11 sub-member in the study area are between 51% and 75%, 71.6% on average (Fig. 21). The study area has a maxi-mum horizontal principal stress of 24.2-71.6 MPa, a minimum horizontal principal stress of 16.0-51.6 MPa, and a horizontal stress difference of 4.1-17.6 MPa. Laterally, the anticline uplift has lower horizontal stress difference, and the syncline trough has higher horizontal stress difference (Fig. 22). Overall, the horizontal stress difference increases with the increase of burial depth. Putting all these together, we concluded that the shale gas reservoirs in Taiyang anticline area are favorable for SRV fracturing, and the shale layers can be easily "crushed" during hydraulic fracturing, forming man-made fractured gas reservoirs.

Fig. 21.   Distribution of brittle mineral content of Wufeng Fm.- the Long-11 sub-member in the study area.


Fig. 22.   Diagram of predicted horizontal stress difference of Wufeng Fm.-Long-11 sub-member in the study area.


In summary, the Taiyang anticline area in the Zhaotong demonstration zone has superior conditions for shallow shale gas enrichment and accumulation. The sweet spot area has advantages in five aspects: a) Favorable sedimentary environment for high-quality shale. Silicon-rich and carbon-rich, high silicon and carbon content, and high silicon and medium carbon content shale developed in the deep-water continental shelf anaerobic environment has a continuous thickness of more than 30 m, indicating favorable shale source and reservoir conditions. b) High-quality shale reservoirs. The shale layers have a lot of organic pores and micro-fractures, good physical properties, and are largely Type I reservoirs favorable for shale gas storage and enrichment. c) The roof and floor of the gas-rich shale reservoirs depositing continuously with the shale reservoirs have tight lithology, large thickness, stable distribution, high breakthrough pressure, and good sealing performance, providing favorable shale gas sealing and preservation conditions. The structure has weak deformation and reformation. The faults under continuous compression have good lateral sealing performance. The anticline has favorable 3D sealing performance and contains typical anticline shale gas reservoir under compression-shear. d) The gas-rich shale sections have higher gas content, and are all in an overpressure state and high in exploration potential, providing the resource base for high production. e) Gas-rich shale layers have high brittle mineral content, and the anticline area has smaller the horizontal stress difference, which are favorable engineering conditions for fracturing to make high yield man-made gas reservoir, and complex fracture network is likely to be formed to realize SRV.

Based on the available criterion of selecting marine shale gas areas in South China[25,26], and according to the recent data of drilling and production pilot in the shallow shale gas reservoirs of the Taiyang anticline area, the criterion of shallow shale gas area selection in Zhaotong demonstration zone has been summarized, as shown in Table 5.

Table 5   Criterion of shallow shale gas sweet spot selection in Zhaotong demonstration zone.

TypeTOC>2% shale thickness/mTotal porosity/
%
Total gas content/
(m3•t-1)
Shale gas reservoir pressure coefficientBrittle indexCaprock conditions of
shale gas reservoirs
Structural
deformation
strength
Regional cap thickness/m
>30>4>41.2-1.6>65Tight lithology, large thickness, stable distribution, and high breakthrough
pressure (marlstone, shale)
Weak (dominated by fold deformation, compressive closed fault)>50
30-102-42-41.2-1.065-50Relatively tight lithology, medium thickness, stable distribution, relatively high breakthrough pressure (tight sandstone, limestone)Medium (folds and faults are relatively developed)<50
<10<2<2<1.0<50Unconsolidated lithology, small thickness, instable distribution, low breakthrough pressure (sandstone, crushed limestone)Strong (open faults, connected to the
surface)
/

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4. Demonstration and technology promotion significance for shallow shale gas exploration

According to statistics of the available data, the buried depth of Wufeng Fm.-Longmaxi Fm. in Zhaotong demonstration zone is shallower than that in the Sichuan Basin, and is mostly between 500-2500 m. The potential shallow shale gas area less than 2 000 m in buried depth is nearly 2 000 km2, and has preliminary estimated resources of over 10 000×108 m3, accounting for nearly half of the total area and resources of the demonstration zone. Hence, PetroChina Zhejiang Oilfield Company deployed shallow geological wells of YQ6, YQ7, and YQ8 in the anticline shallow buried area between Haoba, Luowang, and Hualang synclines in the middle of Zhaotong demonstration zone (Fig. 23) in August 2018. It has been confirmed by drilling that the shallow shale gas reservoirs are well developed, and have good gas display and rich resources, and are the key domain for the next step of shale gas exploration and development in the demonstration zone, and they have become hot spots for exploration and evaluation of shallow shale gas sweet spots in the near future. In June 2019, two shallow shale gas evaluation vertical wells YS137 and YS203 drilled on the north and south flanks of the Haiba anticline in the south of the Taiyang anticline area made major breakthroughs. The shale gas reservoirs in them at the depth of 1032 m and 1643 m respectively were tested a gas production of over 4.4×104 m3/d and 4.2×104 m3/d respectively after fracturing, demonstrating bright prospect of shallow shale gas exploration in the demonstration zone.

Fig. 23.   Correlation of Wufeng Fm.-Longmaxi Fm. shale in the central Zhaotong demonstration zone.


In summary, the sweet spot selection method and exploration technology in shallow shale gas reservoir through pilot of shallow shale gas drilling, fracturing, and productivity evaluation in Zhaotong demonstration zone has not only promoted the technological progress of shale gas exploration and development in the demonstration zone, but also boosted the commercial development of marine shale gas in Yunnan, Guizhou and Guangxi, and played a leading role in technical popularization and demonstration in the Yangtze River Economic Belt. According to the preliminary shale gas evaluation, the marine shale gas prospective area in the complex structure residual basin of the Yangtze River Economic Belt has an acreage of around 15×104 km2 and estimated resources of (16.70-18.15)×1012 m3. In Junlian of south Sichuan, Xishui of Guizhou, Qianjiang of Chongqing, and Yichang of Hubei, active shale gas shows have been found at the buried depths of 156-1453 m, and some geological survey wells have tested thousands of cubic meters of production after fracturing, indicating promising prospect of shallow shale gas exploration.

5. Conclusions

Sedimentary environment is the main factor controlling shallow shale gas “source and reservoir”, which are the geological basis for hydrocarbon generation. In the Caledonian period, the Taiyang anticline area in Zhaotong demonstration zone in the southeastern edge of the Upper Yangtze region entered the sedimentary environment of anaerobic foreland basin occlusion bay in the deep-water shelf, and received thick siliceous shale and carbonaceous shale sediments. The shale of Wufeng Fm.-Long-11 sub-member has TOC of more than 2%, and an average measured porosity of 4.98%, and is in the stage of over-maturity dry gas (with an average vitrinite reflectance of 2.41%). All these show the study area has good shale source and reservoir conditions and is a favorable exploration area for shallow shale gas.

The main target reservoir has regional cap, the roof and floor of the reservoir are tight and have good sealing performance, and the structure has suffered weak reformation after deposition, these are prerequisites for preservation of shallow shale gas in the demonstration zone. Exploration practice proves that the stable area with relatively weak structural reformation (trough-like structural belt) in the central and northern part of Zhaotong demonstration zone is the favorable area for shallow shale gas exploration.

The shallow shale gas in the high-yield and gas-rich region of the Taiyang anticline has enriched in the typical compression-shear reformed trap model. This area has Type I reservoirs, high gas content, formation overpressure, high brittle mineral content, slightly lower horizontal stress difference, and good reservoir quality, which are favorable for gas enrichment and accumulation, and creating man-made fracture-type gas reservoirs by volume fracturing.

The distribution and enrichment of shallow shale gas sweet spot and high-yield areas in the demonstration zone are controlled by lithofacies in the sedimentary period, deformation strength in the reformation period, and sealing in the reservoir-forming period. The silicon-rich and carbon-rich shale depositing in the anoxic deep-water continental shelf is the main factor controlling development of shallow shale gas source and reservoir. The anticline structure with weak structural deformation and closed faults and the wide and gentle syncline provide favorable conditions for shallow shale gas enrichment and accumulation. The 3D sealing system of regional cap+ roof and floor is a key factor for shallow shale gas accumulation.

In South China complex structure area outside the Sichuan Basin, the paleozoic marine shale gas shows considerable exploration potential and is a key area of realizing breakthroughs in marine shale gas exploration in South China. The breakthroughs in shallow shale gas exploration and the innovative practice of productivity construction and core technologies in the Zhaotong demonstration zone will play a demonstration and leading role in shale gas development.

Nomenclature

c—compaction coefficient of normal compacted mudstone, m-1;

g—gravitational acceleration, 9.8 m/s2;

GR—natural gamma, API;

pz—pore pressure or formation pressure of undercompacted mudstone, Pa;

Rd—resistivity, Ω·m;

Ro—vitrinite reflectance, %;

TOC—total organic carbon content, %;

z—buried depth of under-compacted mudstone, m;

ρr— average density of sedimentary rock, kg/m3;

ρw—the density of pore water in the formation, kg/m3;

Δt—interval transit time of under-compacted mudstone, μs/m;

Δt0—interval transit time of original surface acoustic wave, μs/m.

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